trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

Base Information

Chemical Name:trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline
CAS No.:137517-69-2
Molecular Formula:C₁₇H₂₃NO
Molecular Weight:257.376
Hs Code.:

Synonyms:trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

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Technology Process of trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

There total 9 articles about trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3,4-diallyl-4-(3-methoxy-phenyl)-1-methyl-piperidine

: 137517-69-2
trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

Guidance literature:: With Grubbs catalyst first generation; In 1,2-dichloro-ethane; at 60 ℃;
DOI:10.1021/ol016588b

Reference yield: 61.0%

: 137517-93-2
(+/-)-2,3,4,4a,5,8-hexahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

: 137517-69-2
cis-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

: 137517-69-2
trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

Guidance literature:: With sodium tetrahydroborate; methanesulfonic acid; In methanol; Title compound not separated from byproducts; 1.) from -60 to 25 deg C, 5 min, 2.) RT, 30 min;
DOI:10.1021/jm00079a005

Reference yield: 61.0%

: 137517-93-2
(+/-)-2,3,4,4a,5,8-hexahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

: 137517-69-2
cis-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

: 137517-69-2
trans-1,2,3,4,4a,5,8,8a-octahydro-4a-(3-methoxyphenyl)-2-methylisoquinoline

Guidance literature:: With sodium tetrahydroborate; methanesulfonic acid; In methanol; Title compound not separated from byproducts; 1.) from -60 to 25 deg C, 5 min, 2.) RT, 30 min;
DOI:10.1021/jm00079a005