1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride

Base Information

• Chemical Name: 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride
• CAS No.: 1446520-84-8
• Molecular Formula: C₂₉H₄₁N₂*Cl
• Molecular Weight: 453.111
• Mol file: 1446520-84-8.mol

Synonyms:1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride

Chemical Property of 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride

There total 4 articles about 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N,N’-bis(4-tert-butylbenzyl)-1,2-cyclohexanediamine (1269602-56-3) + orthoformic acid triethyl ester (122-51-0) → 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride (1446520-84-8)

Guidance literature:

With ammonium chloride; at 110 ℃; Inert atmosphere; Schlenk technique;

DOI:10.3987/COM-13-12678

Reference yield:

rac-diaminocyclohexane (694-83-7) → 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride (1446520-84-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 13.5 h / 20 °C / Reflux

3: ammonium chloride / 110 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; ammonium chloride; In methanol; ethanol;

DOI:10.3987/COM-13-12678

Reference yield:

4-tert-Butylbenzaldehyde (939-97-9) → 1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazolinium chloride (1446520-84-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 13.5 h / 20 °C / Reflux

3: ammonium chloride / 110 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; ammonium chloride; In methanol; ethanol;

DOI:10.3987/COM-13-12678

upstream raw materials:

N,N’-bis(4-tert-butylbenzyl)-1,2-cyclohexanediamine

orthoformic acid triethyl ester

rac-diaminocyclohexane

4-tert-Butylbenzaldehyde