2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Base Information

Chemical Name:2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)
CAS No.:1227255-67-5
Molecular Formula:C₂₆H₃₈N₄O₄
Molecular Weight:470.612
Hs Code.:

Synonyms:2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Suppliers and Price of 2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of 2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

There total 4 articles about 2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 66-98-8
4,4'-diformylbiphenyl

: 1227255-67-5
2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Guidance literature:: In toluene; for 3h; Reflux; Inert atmosphere;
DOI:10.1021/cg201224g

Reference yield:

: 92-86-4
4-(4-bromophenyl)bromobenzene

: 1227255-67-5
2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / 0.92 h / -78 - -50 °C / Inert atmosphere; Sealed tube

1.2: 1 h / -78 °C / Inert atmosphere; Sealed tube

2.1: toluene / Inert atmosphere; Reflux

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; toluene;
DOI:10.1039/c7tc03357e

Reference yield:

: 10602-01-4
p-bromobenzaldehyde 1,3-dioxolane

: 1227255-67-5
2,2'-(biphenyl-4,4'-diyl)bis(4,4,5,5-tetramethylimidazolidine-1,3-diol)

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 24 h / Reflux

1.2: 72 h / Reflux

2.1: toluene / 3 h / Reflux; Inert atmosphere

With magnesium; In tetrahydrofuran; toluene;
DOI:10.1021/cg201224g