3-phenylsydnone

Base Information

Chemical Name:3-phenylsydnone
CAS No.:76458-13-4
Molecular Formula:C₁₃H₁₂N₄O₂
Molecular Weight:256.264
Hs Code.:

3-<p-(3',5'-dimethyl-1'-pyrazolyl)>phenylsydnone

Synonyms:3-phenylsydnone

Suppliers and Price of 3-phenylsydnone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenylsydnone

Chemical Property:

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Technology Process of 3-phenylsydnone

There total 4 articles about 3-phenylsydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-24-7
acetic anhydride

: 76458-04-3
C₁₃H₁₄N₄O₃

: 76458-13-4
3-phenylsydnone

Guidance literature:: at 100 ℃; for 3h;
DOI:10.1002/jhet.5570170538

Reference yield:

: 52708-32-4
3,5-dimethyl-1-(4'-aminophenyl)-1H-pyrazole

: 76458-13-4
3-phenylsydnone

Guidance literature:: Multi-step reaction with 4 steps

1: Sodium acetate / ethanol / 25 h / 130 °C

2: 10percent aq. NaOH

3: Sodium nitrite / H₂O / 0.5 h / 0 - 5 °C

4: 75 percent / 3 h / 100 °C

With sodium hydroxide; sodium acetate; sodium nitrite; In ethanol; water;
DOI:10.1002/jhet.5570170538

Reference yield:

: 76457-96-0
[4-(3,5-Dimethyl-pyrazol-1-yl)-phenylamino]-acetic acid

: 76458-13-4
3-phenylsydnone

Guidance literature:: Multi-step reaction with 2 steps

1: Sodium nitrite / H₂O / 0.5 h / 0 - 5 °C

2: 75 percent / 3 h / 100 °C

With sodium nitrite; In water;
DOI:10.1002/jhet.5570170538