tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate
CAS No.:1400642-75-2
Molecular Formula:C₂₂H₃₄N₂O₃
Molecular Weight:374.524
Hs Code.:

Synonyms:tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

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Technology Process of tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

There total 1 articles about tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 52853-55-1
N-benzyl(2-methylallyl)amine

: 147804-30-6
1-oxa-6-aza-spiro-[2.5]octane-6-caboxylic acid tert-butyl ester

: 1400642-75-2
tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

Guidance literature:: In ethanol; at 80 ℃; for 16h; Sealed vial;

Reference yield:

: 1400642-75-2
tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

: 1400642-77-4
tert-butyl 4-benzyl-2,2-dimethyl-1-oxa-4,9-diazaspiro[5.5]undecane-9-carboxylate

Guidance literature:: tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate; With iodine; sodium hydrogencarbonate; In tert-butyl methyl ether; water; for 16h;

With sodium tetrahydroborate; In dimethyl sulfoxide; at 100 ℃; for 4h;

Reference yield:

: 1400642-75-2
tert-butyl 4-[[benzyl(2-methylallyl)amino]methyl]-4-hydroxy-piperidine-1-carboxylate

: 1400642-79-6
1-(8-benzyl-10,10-dimethyl-11-oxa-3,8-diazaspiro[5.5]undecan-3-yl)-2,2,2-trifluoro-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; iodine / water; tert-butyl methyl ether / 16 h

1.2: 4 h / 100 °C

2.1: hydrogenchloride / 1,4-dioxane; ethanol / 0.5 h

2.2: pH 13 - 14

3.1: pyridine / dichloromethane / 16 h / -78 - 20 °C

With pyridine; hydrogenchloride; iodine; sodium hydrogencarbonate; In 1,4-dioxane; ethanol; dichloromethane; tert-butyl methyl ether; water;