(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

Base Information

Chemical Name:(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone
CAS No.:1162259-93-9
Molecular Formula:C₁₈H₁₇NO₄
Molecular Weight:311.337
Hs Code.:

Synonyms:(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

Chemical Property:

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Technology Process of (3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

There total 6 articles about (3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₃NO₄

: 1162259-93-9
(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 70 ℃; under 52505.3 Torr;

Reference yield:

: 168619-23-6
methyl 3-benzyloxy-5-{[trifluoromethylsulfonyl]oxy}benzoate

: 1162259-93-9
(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 5 h / Heating / reflux

2: water; sodium hydroxide / 1,4-dioxane / 20 °C

3: 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / acetonitrile / 12 h / 20 °C

4: hydrogen / palladium on activated charcoal / tetrahydrofuran / 70 °C / 52505.3 Torr

With 4-methyl-morpholine; water; hydrogen; sodium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile; 1: Suzuki Coupling;

Reference yield:

: 1162259-91-7
3-benzo[1,3]dioxol-5-yl-5-benzyloxy-benzoic acid methyl ester

: 1162259-93-9
(3-benzo[1,3]dioxol-5-yl-5-hydroxy-phenyl)-pyrrolidin-1-yl-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / 1,4-dioxane / 20 °C

2: 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / acetonitrile / 12 h / 20 °C

3: hydrogen / palladium on activated charcoal / tetrahydrofuran / 70 °C / 52505.3 Torr

With 4-methyl-morpholine; water; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; acetonitrile;