C₃₅H₂₆N₂O₈

Base Information

Chemical Name:C₃₅H₂₆N₂O₈
CAS No.:144019-96-5
Molecular Formula:C₃₅H₂₆N₂O₈
Molecular Weight:602.6
Hs Code.:

C<sub>35</sub>H<sub>26</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₅H₂₆N₂O₈

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Chemical Property of C₃₅H₂₆N₂O₈

Chemical Property:

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Technology Process of C₃₅H₂₆N₂O₈

There total 17 articles about C₃₅H₂₆N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108-24-7
acetic anhydride

: 144041-66-7
C₃₃H₂₄N₂O₇

: 144019-96-5
C₃₅H₂₆N₂O₈

Guidance literature:: With pyridine; dmap; at 25 ℃; for 2h;
DOI:10.1021/ja00049a023

Reference yield:

: 144019-65-8
3-(benzyloxy)-7,8,9,10-tetrahydrophenanthridine

: 144019-96-5
C₃₅H₂₆N₂O₈

Guidance literature:: Multi-step reaction with 14 steps

1: 88 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

2: 80 percent / 14 h / 25 °C

3: 98 percent / K₂CO₃ / methanol / 2 h / 25 °C

4: 98 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 25 °C

5: 89 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr

6: 1.) NaH, 2.) n-Bu₄NI / 1.) THF, 10 min, 2.) THF, 25 deg C, 1 h

7: 98 percent / tetrahydrofuran / 0.25 h / -78 - 0 °C

8: 1.) Pd(PPh₃)4, n-PrNH₂, 2.) CuI / 1.) benzene, 25 deg C, 15 min, 2.) benzene, 25 deg C, 5 h

9: m-CPBA / CH₂Cl₂ / 1 h / 25 °C

10: 82 percent / 48percent aq. HBr / tetrahydrofuran / 2 h / 25 °C

11: 1.) AgNO₃, 2.) KCN / 1.) THF, EtOH, H₂O, 25 deg C, 1 h, 2.) THF, EtOH, H₂O, 25 deg C, 10 min

12: 59 percent / sat. aq. NaHCO₃, m-CPBA / CH₂Cl₂ / 1 h / 25 °C

13: 42 percent / LDA / toluene; cyclohexane / 0.33 h / -78 °C

14: 77 percent / DMAP, pyridine / 2 h / 25 °C

With pyridine; 2,6-dimethylpyridine; propylamine; dmap; potassium cyanide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; toluene;
DOI:10.1021/ja00049a023

Reference yield:

: 144019-57-8
N-(3-hydroxyphenyl)-1,4-dioxaspiro<4.5>decane-6-carboxamide

: 144019-96-5
C₃₅H₂₆N₂O₈

Guidance literature:: Multi-step reaction with 16 steps

1: 1.) NaH, 2.) tetra-n-butylammonium iodide / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 1 h

2: 1.) 37percent aq. HCl, 2.) DIBAL, LiAlH₄, 3.) silica gel, O₂

3: 88 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

4: 80 percent / 14 h / 25 °C

5: 98 percent / K₂CO₃ / methanol / 2 h / 25 °C

6: 98 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 25 °C

7: 89 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr

8: 1.) NaH, 2.) n-Bu₄NI / 1.) THF, 10 min, 2.) THF, 25 deg C, 1 h

9: 98 percent / tetrahydrofuran / 0.25 h / -78 - 0 °C

10: 1.) Pd(PPh₃)4, n-PrNH₂, 2.) CuI / 1.) benzene, 25 deg C, 15 min, 2.) benzene, 25 deg C, 5 h

11: m-CPBA / CH₂Cl₂ / 1 h / 25 °C

12: 82 percent / 48percent aq. HBr / tetrahydrofuran / 2 h / 25 °C

13: 1.) AgNO₃, 2.) KCN / 1.) THF, EtOH, H₂O, 25 deg C, 1 h, 2.) THF, EtOH, H₂O, 25 deg C, 10 min

14: 59 percent / sat. aq. NaHCO₃, m-CPBA / CH₂Cl₂ / 1 h / 25 °C

15: 42 percent / LDA / toluene; cyclohexane / 0.33 h / -78 °C

16: 77 percent / DMAP, pyridine / 2 h / 25 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; propylamine; dmap; potassium cyanide; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; hydrogen; oxygen; silica gel; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; toluene;
DOI:10.1021/ja00049a023