3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

Base Information

Chemical Name:3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione
CAS No.:713143-69-2
Molecular Formula:C₂₄H₃₇NO₄
Molecular Weight:403.562
Hs Code.:

Synonyms:3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

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Chemical Property of 3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

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Technology Process of 3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

There total 1 articles about 3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (E)-(3S,6R,8S,11S,13S)-3-Benzyl-13-[2-(4-methoxy-benzyloxy)-ethyl]-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridec-9-ene-2,5-dione

: 713143-69-2
3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 8h; under 760 Torr;
DOI:10.1002/anie.200453663

Reference yield: 82.0%

: 713143-69-2
3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

: 713143-84-1
(3S,6R,8R,11R,13S)-3-Benzyl-13-(2-iodo-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.333333h;
DOI:10.1002/anie.200453663

Reference yield:

: 713143-69-2
3-benzyl-13-(2-hydroxy-ethyl)-4,6,8,11-tetramethyl-1-oxa-4-aza-cyclotridecane-2,5-dione

: 713143-96-5
4-((3S,6R,8R,11R,13R)-3-Benzyl-4,6,8,11-tetramethyl-2,5-dioxo-1-oxa-4-aza-cyclotridec-13-yl)-butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / I₂; imidazole; triphenylphosphine / tetrahydrofuran / 0.33 h / 20 °C

2: 85 percent / 2,2'-azobisisobutyronitrile / benzene / 4 h / Heating

3: 87 percent / K₂OsO₄*2H₂O; NaIO₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

With 1H-imidazole; potassium osmate(VI); sodium periodate; 2,2'-azobis(isobutyronitrile); iodine; triphenylphosphine; In tetrahydrofuran; water; benzene;
DOI:10.1002/anie.200453663