C₄₃H₄₄N₂O₇

Base Information

Chemical Name:C₄₃H₄₄N₂O₇
CAS No.:1338645-88-7
Molecular Formula:C₄₃H₄₄N₂O₇
Molecular Weight:700.832
Hs Code.:

C<sub>43</sub>H<sub>44</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₄₃H₄₄N₂O₇

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Chemical Property of C₄₃H₄₄N₂O₇

Chemical Property:

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Technology Process of C₄₃H₄₄N₂O₇

There total 12 articles about C₄₃H₄₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1338645-87-6
C₄₄H₄₄N₂O₅

: 1338645-88-7
C₄₃H₄₄N₂O₇

Guidance literature:: C₄₄H₄₄N₂O₅; With 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate; In tetrahydrofuran; water; for 0.166667h;

With osmium(VIII) oxide; In tetrahydrofuran; water; toluene;
DOI:10.1021/ol202573s

Reference yield:

: C₂₉H₃₃NO₄

: 1338645-88-7
C₄₃H₄₄N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1: sodium periodate / acetone; toluene / 0.5 h

2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

4: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

With 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 2: Pinnick oxidation;
DOI:10.1021/ol202573s

Reference yield:

: C₂₆H₂₇NO₃

: 1338645-88-7
C₄₃H₄₄N₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / dichloromethane; toluene / -78 - 0 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 - 0 °C

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; toluene / 5 h

4: sodium periodate / acetone; toluene / 0.5 h

5: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

7: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; boron trifluoride diethyl etherate; water; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 5: Pinnick oxidation;
DOI:10.1021/ol202573s