14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione

Base Information

• Chemical Name: 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione
• CAS No.: 785042-21-9
• Molecular Formula: C₅₀H₆₈N₄O₄
• Molecular Weight: 789.114

Synonyms:14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione

Chemical Property of 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione

Chemical Property:

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Technology Process of 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione

There total 8 articles about 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.2^2,5]octatriaconta-1⁽³⁵⁾,2⁽³⁸⁾,3,5⁽³⁷⁾,32⁽³⁶⁾,33-hexaene-13,24-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(tert-butoxycarbonylamino)hexanoic acid (6404-29-1) → 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.22,5]octatriaconta-1(35),2(38),3,5(37),32(36),33-hexaene-13,24-dione (785042-21-9)

Guidance literature:

Multi-step reaction with 5 steps

1: Et₃N / dioxane / 0.5 h

2: dioxane / 20 °C

3: TFA / 12 h / 20 °C

4: 3 Angstroem molecular sieves / ethanol / 72 h / 20 °C

5: NaBH₄ / ethanol / 12 h / 20 °C

With sodium tetrahydroborate; 3 A molecular sieve; triethylamine; trifluoroacetic acid; In 1,4-dioxane; ethanol;

DOI:10.1021/jm020835f

Reference yield:

(6Z,30Z)-14,23-Bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.22,5]octatriaconta-1(35),2(38),3,5(37),6,30,32(36),33-octaene-13,24-dione → 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.22,5]octatriaconta-1(35),2(38),3,5(37),32(36),33-hexaene-13,24-dione (785042-21-9)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 12h;

DOI:10.1021/jm020835f

Reference yield:

1,8-diaminooctan (373-44-4) → 14,23-bis-(2-methoxy-benzyl)-7,14,23,30-tetraaza-tricyclo[30.2.2.22,5]octatriaconta-1(35),2(38),3,5(37),32(36),33-hexaene-13,24-dione (785042-21-9)

Guidance literature:

Multi-step reaction with 6 steps

1: toluene / 3 h / Heating

2: NaBH₄ / ethanol / 12 h / 20 °C

3: dioxane / 20 °C

4: TFA / 12 h / 20 °C

5: 3 Angstroem molecular sieves / ethanol / 72 h / 20 °C

6: NaBH₄ / ethanol / 12 h / 20 °C

With sodium tetrahydroborate; 3 A molecular sieve; trifluoroacetic acid; In 1,4-dioxane; ethanol; toluene;

DOI:10.1021/jm020835f

upstream raw materials:

1,8-diaminooctan

6-(tert-butoxycarbonylamino)hexanoic acid

ortho-anisaldehyde

C₁₄H₂₅NO₆

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