methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

Base Information

Chemical Name:methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate
CAS No.:1202704-54-8
Molecular Formula:C₁₉H₁₉ClN₂O₈
Molecular Weight:438.821
Hs Code.:

Synonyms:methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

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Chemical Property of methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

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Technology Process of methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

There total 1 articles about methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: methyl 1-[(2-chlorophenyl)methyl]-4,6-dihydroxy-2-oxo-1,2-dihydro-5-pyridinecarboxylate

: 2949-22-6
Glycine ethyl ester isocyanate

: 1202704-54-8
methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 120 ℃; for 0.75h; Microwave irradiation; Sealed flask;

Reference yield: 83.0%

: 1202704-54-8
methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

: 102-49-8
3,4-dichlorobenzyl amine

: 1202698-60-9
N-{[1-[(2-chlorophenyl)methyl]-5-({[(3,4-dichlorophenyl)methyl]amino}carbonyl)-4,6-dihydroxy-2-oxo-1,2-dihydro-3-pyridinyl]carbonyl}glycine

Guidance literature:: methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate; 3,4-dichlorobenzyl amine; In 1,4-dioxane; at 150 ℃; for 0.5h; Microwave irradiation; Sealed tube;

With sodium hydroxide; In ethanol;

With hydrogenchloride; In water; ethyl acetate;

Reference yield: 74.4%

: 107-10-8,42939-71-9
propylamine

: 1202704-54-8
methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate

: 1202700-05-7
N-({1-[(2-chlorophenyl)methyl]-4,6-dihydroxy-2-oxo-5-[(propylamino)carbonyl]-1,2-dihydro-3-pyridinyl}carbonyl)glycine

Guidance literature:: propylamine; methyl 1-[(2-chlorophenyl)methyl]-5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1,6-dihydro-3-pyridinecarboxylate; In chloroform; at 150 ℃; for 0.5h; Microwave irradiation;

With sodium hydroxide; In ethanol; at 20 ℃;

With hydrogenchloride; In ethanol; water; ethyl acetate;