[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

Base Information

Chemical Name:[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol
CAS No.:130217-48-0
Molecular Formula:C₁₄H₂₂Cl₂O₂Si
Molecular Weight:321.319
Hs Code.:

Synonyms:[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

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Chemical Property of [2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

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Technology Process of [2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

There total 1 articles about [2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56962-08-4
4,5-dichlorophthalic acid

: 130217-48-0
[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / LiAlH₄ / tetrahydrofuran / 16 h / Ambient temperature

2: triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / Ambient temperature

With dmap; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield: 86.0%

: 130217-48-0
[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1211937-21-1
C₂₁H₂₆Cl₂N₄OSSi

Guidance literature:: 1-Phenyl-1H-tetrazole-5-thiol; With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200904527

Reference yield: 44.0%

: 3607-17-8
3-bromopropyltriphenylphosphonium bromide

: 130217-48-0
[2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol

: 1000597-04-5
C₁₇H₂₄Cl₂OSi

Guidance literature:: [2-(tert-Butyl-dimethyl-silanyloxymethyl)-4,5-dichloro-phenyl]-methanol; With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;

3-bromopropyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; Further stages.; Heating;
DOI:10.1021/ja0746316