1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

Base Information

Chemical Name:1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole
CAS No.:367491-58-5
Molecular Formula:C₃₀H₂₂N₄O
Molecular Weight:454.531
Hs Code.:

1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1<i>H</i>-isoindole

Synonyms:1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

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Chemical Property of 1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

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Technology Process of 1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

There total 6 articles about 1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 367491-57-4
4-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-phthalonitrile

: 367491-58-5
1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

Guidance literature:: With ammonia; In methanol; at 68 ℃; for 8h;
DOI:10.1246/cl.2001.788

Reference yield:

: 696-62-8
para-iodoanisole

: 367491-58-5
1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / K₂CO₃; 18-crown-6; Cu / 9 h / 170 °C

2: 66 percent / BBr₃ / CH₂Cl₂ / 3 h / -78 °C

3: 94 percent / K₂CO₃ / dimethylsulfoxide / 24 h / 25 °C

4: 91 percent / NH₃ / methanol / 8 h / 68 °C

With 18-crown-6 ether; ammonia; boron tribromide; copper; potassium carbonate; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1246/cl.2001.788

Reference yield:

: 31643-49-9
4-Nitrophthalonitrile

: 367491-58-5
1,3-diimino-5-[4-(naphthalen-2-yl-phenyl-amino)-phenoxy]-2,3-dihydro-1H-isoindole

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / dimethylsulfoxide / 24 h / 25 °C

2: 91 percent / NH₃ / methanol / 8 h / 68 °C

With ammonia; potassium carbonate; In methanol; dimethyl sulfoxide;
DOI:10.1246/cl.2001.788