C₃₂H₄₄O₁₀S₂

Base Information

Chemical Name:C₃₂H₄₄O₁₀S₂
CAS No.:890532-97-5
Molecular Formula:C₃₂H₄₄O₁₀S₂
Molecular Weight:652.827
Hs Code.:

C<sub>32</sub>H<sub>44</sub>O<sub>10</sub>S<sub>2</sub>

Synonyms:C₃₂H₄₄O₁₀S₂

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Chemical Property of C₃₂H₄₄O₁₀S₂

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Technology Process of C₃₂H₄₄O₁₀S₂

There total 4 articles about C₃₂H₄₄O₁₀S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 890532-91-9
Toluene-4-sulfonic acid (S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-pent-4-enyl ester

: C₃₂H₄₄O₁₀S₂

: 890532-97-5
C₃₂H₄₄O₁₀S₂

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; at 40 ℃; for 12h;
DOI:10.1016/j.tetlet.2006.03.080

Reference yield:

: 890532-87-3
(S)-1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-pent-4-en-1-ol

: 890532-97-5
C₃₂H₄₄O₁₀S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / TEA; DMAP / CH₂Cl₂ / 24 h / 0 - 20 °C

2: 82 percent / Grubbs' 1^st generation catalyst / CH₂Cl₂ / 12 h / 40 °C

With dmap; TEA; Grubbs catalyst first generation; In dichloromethane;
DOI:10.1016/j.tetlet.2006.03.080

Reference yield:

: 93367-10-3,212375-57-0
(2S,3S)-3,4-epoxy-1,2-di-O-isopropylidenebutane-1,2-diol

: 890532-97-5
C₃₂H₄₄O₁₀S₂

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / CuI / diethyl ether / 12 h / -20 °C

2: 87 percent / TEA; DMAP / CH₂Cl₂ / 24 h / 0 - 20 °C

3: 82 percent / Grubbs' 1^st generation catalyst / CH₂Cl₂ / 12 h / 40 °C

With dmap; copper(l) iodide; TEA; Grubbs catalyst first generation; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2006.03.080