(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

Base Information

Chemical Name:(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione
CAS No.:161745-70-6
Molecular Formula:C₃₀H₃₆N₂O₆
Molecular Weight:520.626
Hs Code.:

Synonyms:(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

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Chemical Property of (2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

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Technology Process of (2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

There total 3 articles about (2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95798-31-5
(4S)-3-(3-phenylpropionyl)-4-(2-propyl)oxazolidin-2-one

: 161815-10-7
(2R,3S)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

: 161745-70-6
(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

Guidance literature:: With titanium tetrachloride; lithium diisopropyl amide; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00110a003

Reference yield:

: 17016-83-0
(4S)-4-isopropyl-1,3-oxazolidin-2-one

: 161745-70-6
(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere; Sealed tube; Schlenk technique

1.2: 2.5 h / -78 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.67 h / -78 °C / Schlenk technique; Inert atmosphere; Sealed tube

2.2: 21 h / 20 °C

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane;

Reference yield:

: 645-45-4
hydrocinnamic acid chloride

: 161745-70-6
(2R,3R)-1,4-bis[(4S)-4-isopropyl-2-oxo(1,3-oxazolidin-3-yl)]-2,3-bisbenzylbutane-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere; Sealed tube; Schlenk technique

1.2: 2.5 h / -78 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.67 h / -78 °C / Schlenk technique; Inert atmosphere; Sealed tube

2.2: 21 h / 20 °C

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane;