tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate

Base Information

• Chemical Name: tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate
• CAS No.: 1241894-33-6
• Molecular Formula: C₃₇H₄₃NO₂
• Molecular Weight: 533.754
• Mol file: 1241894-33-6.mol

Synonyms:tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate

Chemical Property of tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate

There total 1 articles about tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

p-tert-butylphenylboronic acid (123324-71-0) + 4,4’-dibromo-N-(tert-butoxycarbonyl)phenylaniline (197144-27-7) → tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate (1241894-33-6)

Guidance literature:

4,4’-dibromo-N-(tert-butoxycarbonyl)phenylaniline; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 20 ℃; for 0.25h; Inert atmosphere;

p-tert-butylphenylboronic acid; With sodium carbonate; In methanol; water; toluene; at 80 ℃; for 20h;

DOI:10.1039/c001122c

Reference yield: 85.0%

tert-butyl bis(4'-tert-butylbiphenyl-4-yl)carbamate (1241894-33-6) → bis(4'-tert-butylbiphenyl-4-yl)amine (1078705-10-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2.75h; Inert atmosphere;

DOI:10.1039/c001122c

upstream raw materials:

p-tert-butylphenylboronic acid

4,4’-dibromo-N-(tert-butoxycarbonyl)phenylaniline

Downstream raw materials:

bis(4'-tert-butylbiphenyl-4-yl)amine