6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline

Base Information

• Chemical Name: 6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline
• CAS No.: 112129-67-6
• Molecular Formula: C₁₉H₂₇NO₂
• Molecular Weight: 301.429

Synonyms:6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline

Chemical Property of 6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline

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Technology Process of 6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline

There total 1 articles about 6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-(4-methoxybenzyl)-6-methoxy-N-methyl-1,2,3,4-tetrahydroisoquinoline (3423-09-4) → 6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline (112129-67-6)

Guidance literature:

With ammonia; lithium; In tetrahydrofuran; tert-butyl alcohol; for 0.416667h; Heating;

DOI:10.3987/R-1987-03-0713

Reference yield:

6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline (112129-67-6) → 1-(4-Hydroxy-cyclohex-1-enylmethyl)-2-methyl-1,2,3,4,5,6,7,8-octahydro-isoquinolin-6-ol (112129-70-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. KHSO₄ / 0.5 h / Ambient temperature

2: 50 percent / lithium aluminum hydride (LAH) / tetrahydrofuran / 12 h / Heating

With potassium hydrogensulfate; lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.3987/R-1987-03-0713

Reference yield:

6-Methoxy-1-(4-methoxy-cyclohexa-1,4-dienylmethyl)-2-methyl-1,2,3,4,5,8-hexahydro-isoquinoline (112129-67-6) → 2-Methyl-1-(4-oxo-cyclohex-1-enylmethyl)-1,3,4,5,7,8-hexahydro-2H-isoquinolin-6-one (112129-69-8)

Guidance literature:

With potassium hydrogensulfate; for 0.5h; Ambient temperature;

DOI:10.3987/R-1987-03-0713

upstream raw materials:

1-(4-methoxybenzyl)-6-methoxy-N-methyl-1,2,3,4-tetrahydroisoquinoline

Downstream raw materials:

2-Methyl-1-(4-oxo-cyclohex-1-enylmethyl)-1,3,4,5,7,8-hexahydro-2H-isoquinolin-6-one

1-(4-Hydroxy-cyclohex-1-enylmethyl)-2-methyl-1,2,3,4,5,6,7,8-octahydro-isoquinolin-6-ol

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