N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

Base Information

Chemical Name:N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)
CAS No.:1443761-08-7
Molecular Formula:C₅₂H₇₈N₄
Molecular Weight:759.218
Hs Code.:

N<SUP>1</SUP>,N<SUP>1'</SUP>-(dodecane-1,12-diyl)bis(N<SUP>6</SUP>-(2,2-diphenylethyl)hexane-1,6-diamine)

Synonyms:N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

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Technology Process of N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

There total 8 articles about N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1443761-10-1
N,N'-(dodecane-1,12-diyl)bis(6-(2,2-diphenylacetamido)hexanamide)

: 1443761-08-7
N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

Guidance literature:: With borane N-ethyl-N-isopropylaniline complex; In tetrahydrofuran; diethylene glycol dimethyl ether; for 5h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2013.06.044

Reference yield: 36.0%

: C₅₂H₇₄N₄O₂

: 1443761-08-7
N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

Guidance literature:: With borane N-ethyl-N-isopropylaniline complex; In diethylene glycol dimethyl ether; for 12h; Reflux;
DOI:10.1016/j.bmcl.2013.04.063

Reference yield:

: 104807-21-8
dibenzyl ((dodecane-1,12-diylbis(azanediyl))bis(6-oxohexane-6,1-diyl))dicarbamate

: 1443761-08-7
N¹,N^1'-(dodecane-1,12-diyl)bis(N⁶-(2,2-diphenylethyl)hexane-1,6-diamine)

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen bromide / acetic acid / 4 h / 20 °C

2: sodium hydroxide / chloroform / 14 h

3: triethylamine / dichloromethane / 20 °C

4: borane N-ethyl-N-isopropylaniline complex / diethylene glycol dimethyl ether / 12 h / Reflux

With hydrogen bromide; triethylamine; sodium hydroxide; borane N-ethyl-N-isopropylaniline complex; In dichloromethane; chloroform; diethylene glycol dimethyl ether; acetic acid;
DOI:10.1016/j.bmcl.2013.04.063