1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

Base Information

Chemical Name:1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone
CAS No.:124870-65-1
Molecular Formula:C₂₀H₂₂N₂O₃
Molecular Weight:338.406
Hs Code.:

1-(p-anisyl)-4-<N-(p-anisyl)-azomethinyl>-3,3-dimethyl-2-azetidinone

Synonyms:1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

Chemical Property:

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Technology Process of 1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

There total 1 articles about 1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 547-63-7,133320-07-7,67505-84-4
Methyl isobutyrate

: 24978-42-5,24764-91-8
1,4-bis(4'-methoxyphenyl)-1,4-diazabuta-1,3-diene

: 124870-65-1
1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C; 2.) THF, hexane, -70 deg C, 15 min; up to r.t.; r.t., 45 min;
DOI:10.1016/S0040-4020(01)80105-8

Reference yield: 90.0%

: 124870-65-1
1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

: 124870-70-8
1-(4-methoxyphenyl)-3,3-dimethyl-4-oxoazetidine-2-carbaldehyde

Guidance literature:: With hydrogenchloride; In chloroform; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80105-8

Reference yield:

: 124870-65-1
1-(p-anisyl)-4--3,3-dimethyl-2-azetidinone

: 124870-75-3
1-(4-methoxyphenyl)-3,3-dimethyl-4-vinylazetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 5percent HCl / CHCl₃ / 1 h / Ambient temperature

2: 1.) n-BuLi / 1.) THF, hexane, 30 min; 2.) THF, hexane, 50 min

With hydrogenchloride; n-butyllithium; In chloroform;
DOI:10.1016/S0040-4020(01)80105-8