Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

Base Information

Chemical Name:Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis
CAS No.:220094-73-5
Molecular Formula:C₃₇H₅₂N₄O₈
Molecular Weight:680.842
Hs Code.:

Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis<carbamat>

Synonyms:Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

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Chemical Property of Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

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Technology Process of Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

There total 5 articles about Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 34446-64-5,42996-84-9
(E)-3-(4-methoxyphenyl)propenoyl chloride

: 220094-70-2
Di(tert-butyl)-N-<3-<(2-aminoethyl)amino>propyl>-N,N'-(ethan-1,2-diyl)bis

: 220094-73-5
Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

Guidance literature:: With triethylamine; In ethyl acetate; for 22h; Ambient temperature;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2270::AID-HLCA2270>3.0.CO;2-#

Reference yield:

: 142039-01-8
Di(tert-butyl)-N-(3-aminopropyl)-N,N'-(ethan-1,2-diyl)bis

: 220094-73-5
Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / KF/celite / acetonitrile / 72 h / Ambient temperature

2: H₂, aq. NH₃ / Raney-Ni / ethanol / 2068.59 Torr / Ambient temperature

3: 90 percent / Et₃N / ethyl acetate / 22 h / Ambient temperature

With potassium fluoride; ammonium hydroxide; Celite; hydrogen; triethylamine; nickel; In ethanol; ethyl acetate; acetonitrile;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2270::AID-HLCA2270>3.0.CO;2-#

Reference yield:

: 187745-72-8
Di(tert-butyl)-N-(2-cyanoethyl)-N,N'-(ethan-1,2-diyl)bis

: 220094-73-5
Di(tert-butyl)-(E,E)-N-<3-<<3-(4-methoxyphenyl)prop-2-enoyl><2-<<3-(4-methoxyphenyl)prop-2-enoyl>-amino>ethyl>amino>propyl>-N,N'-(ethan-1,2-diyl)bis

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, aq. NH₃ / Raney-Ni / ethanol / 20 h / 2068.59 Torr / Ambient temperature

2: 86 percent / KF/celite / acetonitrile / 72 h / Ambient temperature

3: H₂, aq. NH₃ / Raney-Ni / ethanol / 2068.59 Torr / Ambient temperature

4: 90 percent / Et₃N / ethyl acetate / 22 h / Ambient temperature

With potassium fluoride; ammonium hydroxide; Celite; hydrogen; triethylamine; nickel; In ethanol; ethyl acetate; acetonitrile;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2270::AID-HLCA2270>3.0.CO;2-#