ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

Base Information

Chemical Name:ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate
CAS No.:1443207-44-0
Molecular Formula:C₁₄H₁₂ClF₃O₂
Molecular Weight:304.696
Hs Code.:

Synonyms:ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

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Chemical Property of ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

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Technology Process of ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

There total 1 articles about ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 70090-69-6
1-chloro-4-(prop-2-yn-1-yl)benzene

: 59733-95-8,906512-35-4
ethyl 3,3,3-trifluoromethyl-2-diazopropionate

: 1443207-44-0
ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

Guidance literature:: With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; In toluene; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.04.076

Reference yield: 96.0%

: 1443207-44-0
ethyl 2-(4-chlorobenzyl)-1-(trifluoromethyl)cycloprop-2-enecarboxylate

: 1443207-55-3
(E)-ethyl 2-(4-chlorobenzylidene)-1-(trifluoromethyl)cyclopropanecarboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.04.076