N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine

Base Information

• Chemical Name: N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine
• CAS No.: 950772-37-9
• Molecular Formula: C₂₀H₃₃N₃O₂
• Molecular Weight: 347.501

Synonyms:N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine

Chemical Property of N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine

Chemical Property:

Purity/Quality:

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Technology Process of N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine

There total 3 articles about N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-[trans-4-(ethyloxy)cyclohexyl]-N-[5-(methyloxy)-2-nitrophenyl]-4-piperidinamine (950772-36-8) → N2-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine (950772-37-9)

Guidance literature:

With hydrazine; nickel; In ethanol; at 20 ℃; for 2h;

Reference yield:

1-[trans-4-(ethoxy)cyclohexyl]-4-piperidinamine dihydrochloride → N2-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine (950772-37-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 28 h / 20 - 90 °C

2: hydrazine / nickel / ethanol / 2 h / 20 °C

With N-ethyl-N,N-diisopropylamine; hydrazine; nickel; In ethanol; N,N-dimethyl-formamide;

Reference yield:

2-fluoro-4-methoxy-1-nitro-benzene (446-38-8) → N2-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-4-(methyloxy)-1,2-benzenediamine (950772-37-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 28 h / 20 - 90 °C

2: hydrazine / nickel / ethanol / 2 h / 20 °C

With N-ethyl-N,N-diisopropylamine; hydrazine; nickel; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

1-[trans-4-(ethyloxy)cyclohexyl]-N-[5-(methyloxy)-2-nitrophenyl]-4-piperidinamine

2-fluoro-4-methoxy-1-nitro-benzene

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