C₃₃H₂₄N₂O₇

Base Information

Chemical Name:C₃₃H₂₄N₂O₇
CAS No.:144041-66-7
Molecular Formula:C₃₃H₂₄N₂O₇
Molecular Weight:560.563
Hs Code.:

C<sub>33</sub>H<sub>24</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₃H₂₄N₂O₇

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Chemical Property of C₃₃H₂₄N₂O₇

Chemical Property:

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Technology Process of C₃₃H₂₄N₂O₇

There total 16 articles about C₃₃H₂₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 144019-95-4
N-<(phenyloxy)carbonyl>-6a,10a-epoxy-6-<3(Z)-hexene-1,5-diynyl>-3-<(2-nitrobenzyl)oxy>-10-oxo-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 144041-66-7
C₃₃H₂₄N₂O₇

Guidance literature:: With lithium diisopropyl amide; In cyclohexane; toluene; at -78 ℃; for 0.333333h;
DOI:10.1021/ja00049a023

Reference yield:

: 144019-65-8
3-(benzyloxy)-7,8,9,10-tetrahydrophenanthridine

: 144041-66-7
C₃₃H₂₄N₂O₇

Guidance literature:: Multi-step reaction with 13 steps

1: 88 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

2: 80 percent / 14 h / 25 °C

3: 98 percent / K₂CO₃ / methanol / 2 h / 25 °C

4: 98 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 25 °C

5: 89 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr

6: 1.) NaH, 2.) n-Bu₄NI / 1.) THF, 10 min, 2.) THF, 25 deg C, 1 h

7: 98 percent / tetrahydrofuran / 0.25 h / -78 - 0 °C

8: 1.) Pd(PPh₃)4, n-PrNH₂, 2.) CuI / 1.) benzene, 25 deg C, 15 min, 2.) benzene, 25 deg C, 5 h

9: m-CPBA / CH₂Cl₂ / 1 h / 25 °C

10: 82 percent / 48percent aq. HBr / tetrahydrofuran / 2 h / 25 °C

11: 1.) AgNO₃, 2.) KCN / 1.) THF, EtOH, H₂O, 25 deg C, 1 h, 2.) THF, EtOH, H₂O, 25 deg C, 10 min

12: 59 percent / sat. aq. NaHCO₃, m-CPBA / CH₂Cl₂ / 1 h / 25 °C

13: 42 percent / LDA / toluene; cyclohexane / 0.33 h / -78 °C

With 2,6-dimethylpyridine; propylamine; potassium cyanide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; toluene;
DOI:10.1021/ja00049a023

Reference yield:

: 144019-57-8
N-(3-hydroxyphenyl)-1,4-dioxaspiro<4.5>decane-6-carboxamide

: 144041-66-7
C₃₃H₂₄N₂O₇

Guidance literature:: Multi-step reaction with 15 steps

1: 1.) NaH, 2.) tetra-n-butylammonium iodide / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 1 h

2: 1.) 37percent aq. HCl, 2.) DIBAL, LiAlH₄, 3.) silica gel, O₂

3: 88 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

4: 80 percent / 14 h / 25 °C

5: 98 percent / K₂CO₃ / methanol / 2 h / 25 °C

6: 98 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 25 °C

7: 89 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr

8: 1.) NaH, 2.) n-Bu₄NI / 1.) THF, 10 min, 2.) THF, 25 deg C, 1 h

9: 98 percent / tetrahydrofuran / 0.25 h / -78 - 0 °C

10: 1.) Pd(PPh₃)4, n-PrNH₂, 2.) CuI / 1.) benzene, 25 deg C, 15 min, 2.) benzene, 25 deg C, 5 h

11: m-CPBA / CH₂Cl₂ / 1 h / 25 °C

12: 82 percent / 48percent aq. HBr / tetrahydrofuran / 2 h / 25 °C

13: 1.) AgNO₃, 2.) KCN / 1.) THF, EtOH, H₂O, 25 deg C, 1 h, 2.) THF, EtOH, H₂O, 25 deg C, 10 min

14: 59 percent / sat. aq. NaHCO₃, m-CPBA / CH₂Cl₂ / 1 h / 25 °C

15: 42 percent / LDA / toluene; cyclohexane / 0.33 h / -78 °C

With 2,6-dimethylpyridine; hydrogenchloride; propylamine; potassium cyanide; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; hydrogen; oxygen; silica gel; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; toluene;
DOI:10.1021/ja00049a023