Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

Base Information

Chemical Name:Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester
CAS No.:360072-94-2
Molecular Formula:C₁₇H₁₉F₃O₄
Molecular Weight:344.331
Hs Code.:

Synonyms:Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

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Chemical Property of Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

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Technology Process of Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

There total 6 articles about Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Carbonic acid (Z)-5-phenyl-3-[1-(tetrahydro-pyran-2-yloxy)-cyclopropyl]-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

: 360072-94-2
Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: With methanol; toluene-4-sulfonic acid; at 20 ℃;
DOI:10.1021/ja010504c

Reference yield:

: 90878-19-6
phenethylmagnesium chloride

: 360072-94-2
Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CuBr*DMS / diethyl ether / -70 °C

2: DIBAL-H / diethyl ether / -70 °C

3: CCl₃OCO₂CCl₃; C₅H₅N / CH₂Cl₂ / 20 °C

4: TsOH; MeOH / 20 °C

With pyridine; methanol; copper(I) bromide dimethylsulfide complex; bis(trichloromethyl) carbonate; diisobutylaluminium hydride; toluene-4-sulfonic acid; In diethyl ether; dichloromethane;
DOI:10.1021/ja010504c

Reference yield:

: 2-(1-ethynylcyclopropoxy)tetrahydro-2H-pyran

: 360072-94-2
Carbonic acid (Z)-3-(1-hydroxy-cyclopropyl)-5-phenyl-pent-2-enyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / n-C₄H₉Li / tetrahydrofuran

2: CuBr*DMS / diethyl ether / -70 °C

3: DIBAL-H / diethyl ether / -70 °C

4: CCl₃OCO₂CCl₃; C₅H₅N / CH₂Cl₂ / 20 °C

5: TsOH; MeOH / 20 °C

With pyridine; methanol; n-butyllithium; copper(I) bromide dimethylsulfide complex; bis(trichloromethyl) carbonate; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja010504c