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Technology Process of (3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

Base Information
  • Chemical Name:(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate
  • CAS No.:1011242-97-9
  • Molecular Formula:C44H61O11P
  • Molecular Weight:796.935
  • Hs Code.:
(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

Synonyms:(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

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Chemical Property of (3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate
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Technology Process of (3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

There total 1 articles about (3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(3S,7S,8R,10E,12E,15R,17E,19E)-21-hydroxy-7,15-bis(4-methoxybenzyloxy)-8-methyl-9-oxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate
1011243-16-5

(3S,7S,8R,10E,12E,15R,17E,19E)-21-hydroxy-7,15-bis(4-methoxybenzyloxy)-8-methyl-9-oxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate
1011242-97-9

(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

Guidance literature:
With pyridine-SO3 complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo7024515

Reference yield: 35.0%

(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate
1011242-97-9

(3S,7S,8R,10E,12E,15R,17E,19E)-7,15-bis(4-methoxybenzyloxy)-8-methyl-9,21-dioxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

(2R,6Z,10S,14S,15R,17E)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione
1011243-01-8

(2R,6Z,10S,14S,15R,17E)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

(3Z,5E,7E,10R,12E,14E,17R,18S,22S)-22-ethyl-10,18-bis(4-methoxybenzyloxy)-17-methyloxacyclodocosa-3,5,7,12,14-pentaene-2,16-dione

(3Z,5E,7E,10R,12E,14E,17R,18S,22S)-22-ethyl-10,18-bis(4-methoxybenzyloxy)-17-methyloxacyclodocosa-3,5,7,12,14-pentaene-2,16-dione

(2R,3aS,5aS,6E,10S,14S,15R,17E,18aR,18bR)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione
1011242-98-0

(2R,3aS,5aS,6E,10S,14S,15R,17E,18aR,18bR)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

(2R,3aR,5aR,6E,10S,14S,15R,17E,18aS,18bS)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione
1011242-99-1

(2R,3aR,5aR,6E,10S,14S,15R,17E,18aS,18bS)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

Guidance literature:
With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 23 ℃; for 72h;
DOI:10.1021/jo7024515
upstream raw materials:

(3S,7S,8R,10E,12E,15R,17E,19E)-21-hydroxy-7,15-bis(4-methoxybenzyloxy)-8-methyl-9-oxohenicosa-10,12,17,19-tetraen-3-yl 2-(diethoxyphosphoryl)acetate

Downstream raw materials:

(2R,6Z,10S,14S,15R,17E)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

(2R,3aS,5aS,6E,10S,14S,15R,17E,18aR,18bR)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

(2R,3aR,5aR,6E,10S,14S,15R,17E,18aS,18bS)-10-ethyl-2,14-bis(4-methoxybenzyloxy)-15-methyl-3,3a,10,11,12,13,14,15,18a,18b-decahydro-1H-indeno[5,4-e][1]oxacyclopentadecine-8,16(2H,5aH)-dione

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