methanebis(thiolate), (dibutylamino)-, nickel salt

Base Information

Chemical Name:methanebis(thiolate), (dibutylamino)-, nickel salt
CAS No.:7236-32-0
Molecular Formula:C₁₅H₁₅NO₃
Molecular Weight:257.289
Hs Code.:

Synonyms:

Suppliers and Price of methanebis(thiolate), (dibutylamino)-, nickel salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanebis(thiolate), (dibutylamino)-, nickel salt

Chemical Property:

Vapor Pressure:0.0473mmHg at 25°C
Boiling Point:236.5°C at 760 mmHg
Flash Point:96.8°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methanebis(thiolate), (dibutylamino)-, nickel salt

There total 2 articles about methanebis(thiolate), (dibutylamino)-, nickel salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7275-41-4
3-aziridin-1-yl-2-benzo[1,3]dioxol-5-yl-cyclohex-2-enone

: 7236-32-0
3a-benzo[1,3]dioxol-5-yl-2,3,3a,5,6,7-hexahydro-indol-4-one

Guidance literature:: With sodium iodide; In diethylene glycol dimethyl ether;
DOI:10.1021/ja00990a045

Reference yield:

: 7236-32-0
3a-benzo[1,3]dioxol-5-yl-2,3,3a,5,6,7-hexahydro-indol-4-one

Guidance literature:: Enamin, Erhitzen mit NaJ;
DOI:10.1016/S0040-4039(00)62012-9

Reference yield:

: 7236-32-0
3a-benzo[1,3]dioxol-5-yl-2,3,3a,5,6,7-hexahydro-indol-4-one

: 510-67-8,510-69-0,546-05-4,7679-52-9,7679-55-2,25375-48-8
(+/-)-crinine

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / PtO₂ / ethanol

2: (i) MeOH, (ii) aq. HCl

3: (i) HCl, Et₂O, (ii) Br₂, AcOH, (iii) LiCl, DMF

4: LiAlH₄ / tetrahydrofuran

5: (i) nBuLi, (ii) TsCl

With lithium aluminium tetrahydride; hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00990a045