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C35H46O10

Base Information
  • Chemical Name:C35H46O10
  • CAS No.:1352816-14-8
  • Molecular Formula:C35H46O10
  • Molecular Weight:626.744
  • Hs Code.:
C<sub>35</sub>H<sub>46</sub>O<sub>10</sub>

Synonyms:C35H46O10

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Chemical Property of C35H46O10
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Technology Process of C35H46O10

There total 12 articles about C35H46O10 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1002/anie.201104681
Guidance literature:
Multi-step reaction with 9 steps
1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
3: pyridine; tributylphosphine / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
4: dihydrogen peroxide / dichloromethane; water / 29 h / 20 °C / pH 7 / aq. phosphate buffer
5: cerium(III) chloride heptahydrate; oxalic acid / acetonitrile / 2 h / 20 °C
6: dichloromethane / 1.5 h / 20 °C
7: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
8: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
9: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C
With pyridine; dmap; tributylphosphine; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; oxalic acid; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201104681
Guidance literature:
Multi-step reaction with 11 steps
1.1: o-xylene / 20 h / 165 °C / Inert atmosphere
2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C
2.2: NaBO3*4H2O / 3 h / 20 °C
3.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
5.1: pyridine; tributylphosphine / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
6.1: dihydrogen peroxide / dichloromethane; water / 29 h / 20 °C / pH 7 / aq. phosphate buffer
7.1: cerium(III) chloride heptahydrate; oxalic acid / acetonitrile / 2 h / 20 °C
8.1: dichloromethane / 1.5 h / 20 °C
9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
11.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C
With pyridine; dmap; tributylphosphine; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; oxalic acid; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; o-xylene; water; acetonitrile; 2.1: Hydroboration reaction;
DOI:10.1002/anie.201104681
upstream raw materials:

C50H64O8Si

C50H64O8Si

C50H66O9Si

C52H68O10Si

Downstream raw materials:

C37H51NO11

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