(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

Base Information

Chemical Name:(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide
CAS No.:1613624-75-1
Molecular Formula:C₂₇H₃₃N₃O₅
Molecular Weight:479.576
Hs Code.:

Synonyms:(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

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Chemical Property of (S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

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Technology Process of (S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

There total 3 articles about (S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613624-74-0
(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic acid

: 1613624-75-1
(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 2 h / 0 °C

2: ammonia / methanol / 18 h / 0 - 20 °C

With 4-methyl-morpholine; ammonia; isobutyl chloroformate; In tetrahydrofuran; methanol;

Reference yield:

: C₂₇H₃₁ClN₂O₅

: 1613624-75-1
(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

Guidance literature:: With ammonia; In methanol; at 0 - 20 ℃; for 18h;

Reference yield:

: 1417189-24-2
C₂₈H₃₄N₂O₆

: 1613624-75-1
(S)-4-(4-(4-(benzyloxycarbonylamino)but-1-ynyl)phenyl)-2-(tert-butoxycarbonylamino)butanoic amide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

2: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 2 h / 0 °C

3: ammonia / methanol / 18 h / 0 - 20 °C

With 4-methyl-morpholine; ammonia; water; sodium hydroxide; isobutyl chloroformate; In tetrahydrofuran; methanol;