C₃₄H₅₂O₇Si

Base Information

Chemical Name:C₃₄H₅₂O₇Si
CAS No.:1365336-59-9
Molecular Formula:C₃₄H₅₂O₇Si
Molecular Weight:600.868
Hs Code.:

C<sub>34</sub>H<sub>52</sub>O<sub>7</sub>Si

Synonyms:C₃₄H₅₂O₇Si

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Chemical Property of C₃₄H₅₂O₇Si

Chemical Property:

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Technology Process of C₃₄H₅₂O₇Si

There total 18 articles about C₃₄H₅₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365414-24-9
C₃₄H₅₂O₇Si

: 1365336-59-9
C₃₄H₅₂O₇Si

: C₃₄H₅₂O₇Si

Guidance literature:: C₃₄H₅₂O₇Si; With (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum; In hexane; toluene; at -48 ℃; Inert atmosphere;

With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran; hexane; toluene; at -48 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol202966m

Reference yield:

: 585-70-6
5-bromo-furan-2-carboxylic acid

: 1365336-59-9
C₃₄H₅₂O₇Si

: C₃₄H₅₂O₇Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: borane-THF / tetrahydrofuran / 48 h / 0 - 20 °C / Inert atmosphere

2.1: 1H-imidazole; dmap / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.1: lithium dicyclohexylamide / toluene / 0.17 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / diethyl ether / 1 h / -78 °C / Inert atmosphere

5.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0.55 h / -100 °C / Inert atmosphere

5.2: 7 h / -100 - -78 °C / Inert atmosphere

6.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 20 h / -20 °C / Inert atmosphere

7.1: dmap; triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

8.1: N,N,N,N,N,N-hexamethylphosphoric triamide / Inert atmosphere

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / Inert atmosphere

10.1: dmap / Inert atmosphere

11.1: (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum / hexane; toluene / -48 °C / Inert atmosphere

11.2: -48 °C / Inert atmosphere

With 1H-imidazole; dmap; borane-THF; di-n-butylboryl trifluoromethanesulfonate; (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum; diisobutylaluminium hydride; lithium dicyclohexylamide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene; acetonitrile; 5.1: Aldol reaction / 5.2: Aldol reaction / 11.1: Aldol reaction / 11.2: Aldol reaction;
DOI:10.1021/ol202966m

Reference yield:

: 1352481-38-9
(4S,5S)-5-(benzyloxy)-4-(4-methoxybenzyloxy)hexan-2-one

: 1365336-59-9
C₃₄H₅₂O₇Si

: C₃₄H₅₂O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0.55 h / -100 °C / Inert atmosphere

1.2: 7 h / -100 - -78 °C / Inert atmosphere

2.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 20 h / -20 °C / Inert atmosphere

3.1: dmap; triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide / Inert atmosphere

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / Inert atmosphere

6.1: dmap / Inert atmosphere

7.1: (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum / hexane; toluene / -48 °C / Inert atmosphere

7.2: -48 °C / Inert atmosphere

With dmap; di-n-butylboryl trifluoromethanesulfonate; (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; acetic acid; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: Aldol reaction / 1.2: Aldol reaction / 7.1: Aldol reaction / 7.2: Aldol reaction;
DOI:10.1021/ol202966m