tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

Base Information

Chemical Name:tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane
CAS No.:200571-97-7
Molecular Formula:C₂₈H₄₀O₃Si
Molecular Weight:452.709
Hs Code.:

Synonyms:tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

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Chemical Property of tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

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Technology Process of tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

There total 4 articles about tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1530-32-1
ethyltriphenylphosphonium bromide

: 200571-96-6
(E)-1-(tert-Butyl-diphenyl-silanyloxy)-7,7-dimethoxy-4-methyl-hept-3-en-2-one

: 200571-97-7
tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

: tert-Butyl-[(E)-2-eth-(E)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 23 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(97)10415-4

Reference yield:

: 104846-46-0
(4E)-5-iodo-4-methylpent-4-en-1-ol

: 200571-97-7
tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: HCl

2: 74 percent / n-BuLi / tetrahydrofuran / -78 °C

3: KN(TMS)2, HMPA / tetrahydrofuran / -78 - 23 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; potassium hexamethylsilazane; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10415-4

Reference yield:

: 154698-93-8
2-((tertbutyldiphenylsilyl)oxy)-N-methoxy-N-methylacetamide

: 200571-97-7
tert-Butyl-[(E)-2-eth-(Z)-ylidene-7,7-dimethoxy-4-methyl-hept-3-enyloxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / n-BuLi / tetrahydrofuran / -78 °C

2: KN(TMS)2, HMPA / tetrahydrofuran / -78 - 23 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; potassium hexamethylsilazane; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10415-4