Technology Process of C28H39FN2O2Si
There total 3 articles about C28H39FN2O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
1,2-dimethoxyethane; water;
for 72h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride; N,N-dimethyl-formamide / 16 h / 20 °C / Cooling with ice
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 72 h / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); thionyl chloride; di-isopropyl azodicarboxylate; sodium carbonate; N,N-dimethyl-formamide; triphenylphosphine;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 72 h / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); di-isopropyl azodicarboxylate; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;