4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

Base Information

Chemical Name:4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone
CAS No.:1233735-87-9
Molecular Formula:C₂₁H₂₄N₆O₂S
Molecular Weight:424.527
Hs Code.:

Synonyms:4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

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Chemical Property of 4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

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Technology Process of 4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

There total 1 articles about 4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 79-19-6
thiosemicarbazide

: 78439-83-5
4-[3,4-dimethoxybenzylidene]-1,5-dimethyl-2-phenyl-1,2-dihydropyrazole-3-one

: 1233735-87-9
4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

Guidance literature:: With potassium carbonate; In ethanol; Reflux;
DOI:10.1016/j.saa.2010.03.007

Reference yield: 75.0%

: copper(II) chloride hydrate

: 1233735-87-9
4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

: 1233735-93-7
bis(4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazonato)copper(II)

Guidance literature:: In ethanol; byproducts: H2O, HCl; soln. of ligand and Cu salt mixed, refluxed; concd. at ca 50°C, cooled, filtered, recrystd. (EtOH), dried (vac., CaCl2); elem. anal.;
DOI:10.1016/j.saa.2010.03.007

Reference yield: 72.0%

: zinc(II) chloride hydrate

: 1233735-87-9
4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazone

: 1233735-98-2
bis(4-(3',4'-dimethoxybenzaldehydene)amino-2,3-dimethyl-1-phenyl-3-pyrazolin-5-thiosemicarbazonato)zinc(II)

Guidance literature:: In ethanol; byproducts: H2O, HCl; a hot soln. of Zn salt mixed with a hot soln. of ligand, refluxed; cooled to room temp., filtered, recrystd., washed (EtOH), dried (vac., CaCl2); elem. anal.;
DOI:10.1016/j.saa.2010.03.007