Technology Process of C40H44N2O10SSi
There total 9 articles about C40H44N2O10SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C38H44O10SSi; uracil;
With
N,O-bis-(trimethylsilyl)-acetamide;
In
acetonitrile;
at 55 ℃;
for 1.5h;
With
trimethylsilyl trifluoromethanesulfonate;
In
acetonitrile;
at 0 - 55 ℃;
for 5.5h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / Cooling with ice
2.1: acetic acid / water / 16 h / 20 °C
3.1: sodium periodate / water; 1,4-dioxane / 1 h
4.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice
5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C
6.1: pyridine / Dichlorofluoromethane / 2 h / 20 °C
7.1: acetic acid; sulfuric acid / water / 2 h / 20 °C
8.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C
8.2: 5.5 h / 0 - 55 °C
With
pyridine; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; sodium hydride; acetic acid; triethylamine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; Dichlorofluoromethane; water; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic acid; sulfuric acid / water / 2 h / 20 °C
2.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C
2.2: 5.5 h / 0 - 55 °C
With
N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; acetic acid;
In
water; acetonitrile;
