Technology Process of C29H31ClO9
There total 11 articles about C29H31ClO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux
2: n-butyllithium / tetrahydrofuran; toluene / -78 °C
3: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C
4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C
5: dmap / pyridine; dichloromethane / 20 °C
6: aluminum (III) chloride / dichloromethane / 0 - 20 °C
7: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C
8: toluene-4-sulfonic acid / water; toluene / Reflux
With
triethylsilane; dmap; aluminum (III) chloride; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; methanol; methanesulfonic acid; dichloromethane; water; toluene; acetonitrile;
6: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap / pyridine; dichloromethane / 20 °C
2: aluminum (III) chloride / dichloromethane / 0 - 20 °C
3: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C
4: toluene-4-sulfonic acid / water; toluene / Reflux
With
dmap; aluminum (III) chloride; sodium tetrahydroborate; toluene-4-sulfonic acid;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water; toluene;
2: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032
