4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

Base Information

Chemical Name:4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole
CAS No.:144993-59-9
Molecular Formula:C₂₉H₃₀Cl₃NO₆
Molecular Weight:594.919
Hs Code.:

Synonyms:4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

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Chemical Property of 4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

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Technology Process of 4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

There total 6 articles about 4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4630-06-2,1569-60-4
6-methylhept-5-en-2-ol

: 144993-59-9
4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N, DMAP

2: 1) O₃, 2) DMS

3: 95 percent / 60 °C

4: p-TsOH

With dmap; 2,3-dimercapto-succinic acid; toluene-4-sulfonic acid; ozone; triethylamine;
DOI:10.1016/S0040-4039(00)79111-8

Reference yield:

: 144762-96-9
4-(2',2',2'-Trichloroethylcarbonoyl)pentanal

: 144993-59-9
4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 60 °C

2: p-TsOH

With toluene-4-sulfonic acid;
DOI:10.1016/S0040-4039(00)79111-8

Reference yield:

: 144936-87-8
2-(2',2',2'-Trichloroethylcarbonoyl)-6-methyl-5-heptene

: 144993-59-9
4-<3-Dioxolan-8-(2',2',2'-trichloroethylcarbonoyl)-5-E-nonen>-2,5-diphenyloxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1) O₃, 2) DMS

2: 95 percent / 60 °C

3: p-TsOH

With 2,3-dimercapto-succinic acid; toluene-4-sulfonic acid; ozone;
DOI:10.1016/S0040-4039(00)79111-8