Bis[di-tert-butyl(4-diMethylaMinophenyl)phosphine]palladiuM(0), Pd 16.7%

Base Information

• Chemical Name: Bis[di-tert-butyl(4-diMethylaMinophenyl)phosphine]palladiuM(0), Pd 16.7%
• CAS No.: 1233717-68-4
• Molecular Formula: C₃₂H₅₆N₂P₂Pd
• Molecular Weight: 637.178
• Mol file: 1233717-68-4.mol

Synonyms:bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium⁽⁰⁾

Chemical Property of Bis[di-tert-butyl(4-diMethylaMinophenyl)phosphine]palladiuM(0), Pd 16.7%

Chemical Property:

• Sensitive.: Air Sensitive
• Water Solubility.: Insoluble in water.

Purity/Quality:

97% ^*data from raw suppliers

Bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium(0) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium(0) is used in cross-coupling including sp2-sp3 coupling, especially Suzuki, Negishi-type, Heck, Sonogashira, and Buchwald-Hartwig coupling reactions.

Technology Process of Bis[di-tert-butyl(4-diMethylaMinophenyl)phosphine]palladiuM(0), Pd 16.7%

There total 2 articles about Bis[di-tert-butyl(4-diMethylaMinophenyl)phosphine]palladiuM(0), Pd 16.7% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine (932710-63-9) → bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium(0) (1233717-68-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 0.17 h / 50 °C / Inert atmosphere

2: bis(pinacol)diborane / toluene / 0.5 h / 70 °C / Inert atmosphere

With bis(pinacol)diborane; In toluene;

DOI:10.1002/anie.201210252

Reference yield:

C36H62N2O4P2Pd → bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium(0) (1233717-68-4)

Guidance literature:

With bis(pinacol)diborane; In toluene; at 70 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201210252

Reference yield: 54.0%

bromobenzene (108-86-1,52753-63-6) + bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]palladium(0) (1233717-68-4) → C22H33BrNPPd

Guidance literature:

In pentane; at 70 ℃; for 2h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201812533

upstream raw materials:

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine

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