methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside
CAS No.:1032716-08-7
Molecular Formula:C₃₀H₃₄O₇
Molecular Weight:506.596
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

There total 1 articles about methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1032715-99-3
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-[(methoxycarbonyl)methyl]-β-D-galactopyranoside

: 1032716-08-7
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

Guidance literature:: With lithium hydroxide; In methanol; heating;
DOI:10.1002/chem.200701151

Reference yield: 93.0%

: 1032716-08-7
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

: 1121-31-9
2-mercaptopyridine N-oxide

: 1353646-50-0
C₃₅H₃₇NO₇S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; Darkness; Inert atmosphere;
DOI:10.1039/c1ob06370g

Reference yield:

: 1032716-08-7
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(carboxymethyl)-β-D-galactopyranoside

: 1200958-56-0
C₂₉H₃₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Darkness; Inert atmosphere

2: 2-methylpropan-2-thiol / benzene / 25 °C / Inert atmosphere; UV-irradiation

With dmap; 2-methylpropan-2-thiol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; benzene; 1: Barton reaction;
DOI:10.1039/c1ob06370g