ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

Base Information

Chemical Name:ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate
CAS No.:117424-96-1
Molecular Formula:C₃₁H₃₄O₈S
Molecular Weight:566.672
Hs Code.:

Synonyms:ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

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Chemical Property of ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

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Technology Process of ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

There total 11 articles about ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 128577-78-6
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

: 117424-96-1
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/jm00172a020

Reference yield:

: 5851-37-6
4-(phenylthio)butan-1-ol

: 117424-96-1
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine (TEA) / diethyl ether

2: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

3: 73 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 2 h / 25 °C

With sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jm00172a020

Reference yield:

: 29193-72-4
ethyl 4-(phenylthio)butanoate

: 117424-96-1
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylsulfonyl)butoxy>benzenepropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 24 percent / LiAlH₄ / diethyl ether / 4 h / 25 °C

2: triethylamine (TEA) / diethyl ether

3: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

4: 73 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 2 h / 25 °C

With lithium aluminium tetrahydride; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jm00172a020