(1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene

Base Information

• Chemical Name: (1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene
• CAS No.: 189817-34-3
• Molecular Formula: C₂₀H₁₈O₅S₂
• Molecular Weight: 402.492

Synonyms:(1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene

Chemical Property of (1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene

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Technology Process of (1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene

There total 1 articles about (1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.0^2,4]non-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

benzene oxide (1488-25-1) + (Z)-1,2-bis(phenylsulfonyl)ethene (963-15-5) → (1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.02,4]non-6-ene (189817-34-3)

Guidance literature:

In benzene; at 80 ℃; for 48h;

DOI:10.1021/jo962267f

Reference yield: 90.0%

(1S,2R,4S,5R,8S,9R)-8,9-Bis-benzenesulfonyl-3-oxa-tricyclo[3.2.2.02,4]non-6-ene (189817-34-3) → (7S,8R)-7,8-Bis-benzenesulfonyl-bicyclo[2.2.2]octa-2,5-diene

Guidance literature:

With n-butyllithium; tungsten(VI) chloride; In tetrahydrofuran; hexane; for 24h; Ambient temperature;

DOI:10.1021/jo962267f

upstream raw materials:

benzene oxide

(Z)-1,2-bis(phenylsulfonyl)ethene

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