C₂₆H₅₁NO₄Si₂

Base Information

Chemical Name:C₂₆H₅₁NO₄Si₂
CAS No.:1427215-75-5
Molecular Formula:C₂₆H₅₁NO₄Si₂
Molecular Weight:497.866
Hs Code.:

C<sub>26</sub>H<sub>51</sub>NO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₂₆H₅₁NO₄Si₂

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Chemical Property of C₂₆H₅₁NO₄Si₂

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Technology Process of C₂₆H₅₁NO₄Si₂

There total 6 articles about C₂₆H₅₁NO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427215-66-4
(5R,6R)-6-azido-5-((R)-1-(4-methoxybenzyloxy)propan-2-yl)-2,2,3,3,9,9,10,10-octameth-yl-4,8-dioxa-3,9-disilaundecane

: 1427215-75-5
C₂₆H₅₁NO₄Si₂

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 45 ℃; for 6.5h;
DOI:10.1016/j.tetlet.2013.02.032

Reference yield:

: 212051-35-9
(R)-methyl 3-((4-methoxybenzyl)oxy)-2-methylpropanoate

: 1427215-75-5
C₂₆H₅₁NO₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / toluene; hexane; methanol / 2 h / 20 °C

1.2: 2 h / -78 °C

2.1: diisobutylaluminium hydride / toluene; dichloromethane / 1 h / -78 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2.5 h / -10 - 0 °C

4.1: sodium azide; Trimethylboroxine / N,N-dimethyl-formamide / 18 h / 60 °C

4.2: 0.33 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

6.1: triphenylphosphine / tetrahydrofuran; water / 6.5 h / 45 °C

With sodium azide; Trimethylboroxine; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.2: |Horner-Wadsworth-Emmons Olefination / 6.1: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.02.032

Reference yield:

: 1427215-62-0
methyl (2Z,4S)-5-[(4-methoxybenzyl)oxy]-4-methylpent-2-enoate

: 1427215-75-5
C₂₆H₅₁NO₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / toluene; dichloromethane / 1 h / -78 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2.5 h / -10 - 0 °C

3.1: sodium azide; Trimethylboroxine / N,N-dimethyl-formamide / 18 h / 60 °C

3.2: 0.33 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

5.1: triphenylphosphine / tetrahydrofuran; water / 6.5 h / 45 °C

With sodium azide; Trimethylboroxine; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5.1: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.02.032