[Pd2(dpm)2(μ-I)(CH3)I]BF4

Base Information

Chemical Name:[Pd2(dpm)2(μ-I)(CH3)I]BF4
CAS No.:78274-93-8
Molecular Formula:BF₄*C₅₁H₄₇I₂P₄Pd₂
Molecular Weight:1337.28
Hs Code.:

Synonyms:[Pd2(dpm)2(μ-I)(CH3)I]BF4

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Chemical Property of [Pd2(dpm)2(μ-I)(CH3)I]BF4

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Technology Process of [Pd2(dpm)2(μ-I)(CH3)I]BF4

There total 1 articles about [Pd2(dpm)2(μ-I)(CH3)I]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: tetrafluoroboric acid

: Pd₂((C₆H₅)2PCH₂P(C₆H₅)2)2CH₂I₂

: 78274-93-8
[Pd2(dpm)2(μ-I)(CH3)I]BF4

Guidance literature:: In dichloromethane; water; acetonitrile; 40 % aq. HBF4 added to Pd-complex in CH2Cl2,; after filtration the soln. was allowed to stand for 18 h, evapd. to half its volume, the solid filtered, washed with methanol, recrystd. from CH2Cl2/Et2O; elem. anal.;
DOI:10.1021/ja00403a025

Reference yield: 90.0%

: 78274-93-8
[Pd2(dpm)2(μ-I)(CH3)I]BF4

: 81457-51-4
[Pd2(dpm)2(μ-I)(COCH3)I]BF4

Guidance literature:: With CO; In dichloromethane; under N2 soln. of Pd complex was treated with CO (45 psig); stirring for 5 d; filtration, treatment with MeOH and Et2O; storing at -5°C for sever d; filtration, washing with ether, recrystn. from CH2Cl2/Et2O; elem.anal.;

Reference yield: 70.0%

: ammonium hexafluorophosphate

: 593-75-9,685498-28-6
methyl isocyanate

: 78274-93-8
[Pd2(dpm)2(μ-I)(CH3)I]BF4

: 81457-53-6
[Pd2(dpm)2(μ-CH3C=NCH3)(CNCH3)2](PF6)3

Guidance literature:: In methanol; under N2 soln. of MeNC was added dropwise to suspn. of Pd complex; filtration, addn. of NH4PF6 in MeOH; filtration, washing with MeOH; recrystn. from acetone/Et2O; elem. anal.;