(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

Base Information

Chemical Name:(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate
CAS No.:1343411-19-7
Molecular Formula:C₂₃H₂₇NO₅
Molecular Weight:397.471
Hs Code.:

Synonyms:(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

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Chemical Property of (E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

Chemical Property:

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Technology Process of (E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

There total 4 articles about (E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1343411-18-6
(E)-methyl 2-(2-((2,5-dimethyl-4-propionylphenoxy)methyl)phenyl)-3-methoxyacrylate

: 1343411-19-7
(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

Guidance literature:: With hydroxylamine hydrochloride; In methanol; at 20 ℃; for 3h; Molecular sieve;

Reference yield:

: 1343411-16-4
(E)-methyl 2-(2-((4-(1-hydroxypropyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

: 1343411-19-7
(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: dipyridinium dichromate / dichloromethane / 2 h / 20 °C

2: hydroxylamine hydrochloride / methanol / 3 h / 20 °C / Molecular sieve

With dipyridinium dichromate; hydroxylamine hydrochloride; In methanol; dichloromethane;

Reference yield:

: 117428-49-6
methyl (E)-2-(2-bromomethylphenyl)-3-methoxyacrylate

: 1343411-19-7
(E)-methyl 2-(2-((4-((E)-1-(hydroxyimino)propyl)-2,5-dimethylphenoxy)methyl)phenyl)-3-methoxyacrylate

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / acetonitrile / 3 h / 20 °C

2: tetrahydrofuran / 2 h / -78 °C

3: dipyridinium dichromate / dichloromethane / 2 h / 20 °C

4: hydroxylamine hydrochloride / methanol / 3 h / 20 °C / Molecular sieve

With dipyridinium dichromate; hydroxylamine hydrochloride; caesium carbonate; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;