3-benzyl-5-[4-(dimethylamino)benzylidene]-2-thioxo-4-imidazolidinone

Base Information

Chemical Name:3-benzyl-5-[4-(dimethylamino)benzylidene]-2-thioxo-4-imidazolidinone
CAS No.:386745-21-7
Molecular Formula:C₁₉H₁₉N₃OS
Molecular Weight:337.445
Hs Code.:
Mol file:386745-21-7.mol

Synonyms:5-((Z)-4-dimethylaminobenzylidene)-3-phenylmethyl-2-thiohydantoin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-benzyl-5-[4-(dimethylamino)benzylidene]-2-thioxo-4-imidazolidinone

Chemical Property:

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Technology Process of 3-benzyl-5-[4-(dimethylamino)benzylidene]-2-thioxo-4-imidazolidinone

There total 2 articles about 3-benzyl-5-[4-(dimethylamino)benzylidene]-2-thioxo-4-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100-10-7
4-dimethylamino-benzaldehyde

: 39123-65-4
3-benzyl-2-thioxotetrahydro-4H-imidazol-4-one

: 386745-21-7
5-((Z)-4-dimethylaminobenzylidene)-3-phenylmethyl-2-thiohydantoin

Guidance literature:: With sodium acetate; In acetic acid; for 4h; Heating;

Reference yield:

: 622-78-6
Benzyl isothiocyanate

: 386745-21-7
5-((Z)-4-dimethylaminobenzylidene)-3-phenylmethyl-2-thiohydantoin

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaOH; pyridine / 1 h / 40 °C / pH 9

1.2: 64 percent / conc. HCl / 2 h / Heating

2.1: 75 percent / NaOAc / acetic acid / 4 h / Heating

With pyridine; sodium hydroxide; sodium acetate; In acetic acid;