2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

Base Information

Chemical Name:2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide
CAS No.:213479-24-4
Molecular Formula:C₁₄H₁₃F₃N₂OS
Molecular Weight:314.331
Hs Code.:

Synonyms:2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

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Chemical Property of 2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

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Technology Process of 2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

There total 1 articles about 2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1645-65-4
4-(trifluoromethyl)phenyl isothiocyanate

: 5220-49-5
3-amino-cyclohex-2-enone

: 213479-24-4
2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

Guidance literature:: In acetonitrile; Heating;
DOI:10.1021/jm981028c

Reference yield: 65.0%

: 213479-24-4
2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

: 213479-25-5
3-(4-Trifluoromethyl-phenylamino)-1,5,6,7-tetrahydro-indazol-4-one

Guidance literature:: With hydrazine hydrate; In ethanol; Heating;
DOI:10.1021/jm981028c

Reference yield:

: 213479-24-4
2-Amino-6-oxo-cyclohex-1-enecarbothioic acid (4-trifluoromethyl-phenyl)-amide

: (4,5,6,7-tetrahydro-1H-indazol-3-yl)(4-trifluoromethyl-phenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / hydrazine hydrate / ethanol / Heating

2: 60 percent / LiAlH₄, conc. aq. H₂SO₄ / tetrahydrofuran / 0.25 h / -78 °C

With lithium aluminium tetrahydride; sulfuric acid; hydrazine hydrate; In tetrahydrofuran; ethanol;
DOI:10.1021/jm981028c