[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

Base Information

Chemical Name:[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester
CAS No.:301644-16-6
Molecular Formula:C₂₁H₂₀ClN₃O₂
Molecular Weight:381.862
Hs Code.:

[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[<i>g</i>]indazol-2-yl]-acetic acid ethyl ester

Synonyms:[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

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Chemical Property of [3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

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Technology Process of [3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

There total 2 articles about [3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 6945-92-2
2-hydrazinyl acetic acid ethyl ester hydrochloride

: 125341-78-8
1-tetralone-2-carbothionic acid p-chloro-anilide

: 301644-16-6
[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

Guidance literature:: 2-hydrazinyl acetic acid ethyl ester hydrochloride; With sodium ethanolate; In ethanol; at 20 ℃; for 0.0833333h;

1-tetralone-2-carbothionic acid p-chloro-anilide; With acetic acid; for 12h; Heating;
DOI:10.1016/S0014-827X(00)00055-0

Reference yield:

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 301644-16-6
[3-(4-chloro-phenylamino)-4,5-dihydro-benzo[g]indazol-2-yl]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 20 °C

1.2: 92 percent / dimethylformamide / 4 h / 20 °C

2.1: EtONa / ethanol / 0.08 h / 20 °C

2.2: 58 percent / CH₃COOH / 12 h / Heating

With sodium ethanolate; sodium hydride; In ethanol; N,N-dimethyl-formamide; 1.1: Metallation / 1.2: Addition / 2.1: Metallation / 2.2: Condensation;
DOI:10.1016/S0014-827X(00)00055-0