1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

Base Information

Chemical Name:1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene
CAS No.:108161-95-1
Molecular Formula:C₁₆H₂₈O₅
Molecular Weight:300.395
Hs Code.:

Synonyms:1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

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Chemical Property of 1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

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Technology Process of 1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

There total 6 articles about 1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108161-93-9
[3-(2,6-Dimethoxy-1-methoxymethoxymethyl-cyclohexa-2,5-dienyl)-1-ethyl-propoxy]-trimethyl-silane

: 108161-95-1
1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

Guidance literature:: With potassium fluoride; pH 6.8 buffer; In methanol; for 17h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90577-0

Reference yield:

: 32541-33-6
1-chloro-3-pentanol

: 108161-95-1
1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / NaI / butan-2-one / 48 h / Heating

2: 86 percent / ethyldiisopropylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 97 percent / LiAlH₄ / diethyl ether / 0.25 h / Ambient temperature

5: 95 percent / ethyldiisopropylamine / CH₂Cl₂ / 24 h / Ambient temperature

6: 99 percent / KF, pH 6.8 buffer / methanol / 17 h / Ambient temperature

With potassium fluoride; lithium aluminium tetrahydride; pH 6.8 buffer; N-ethyl-N,N-diisopropylamine; sodium iodide; In methanol; diethyl ether; dichloromethane; butanone;
DOI:10.1016/S0040-4020(01)90577-0

Reference yield:

: 108161-72-4
rac-1-iodo-pentan-3-ol

: 108161-95-1
1-(3'-hydroxypentyl)-2,6-dimethoxy-1-(methoxymethoxymethyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / ethyldiisopropylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 97 percent / LiAlH₄ / diethyl ether / 0.25 h / Ambient temperature

4: 95 percent / ethyldiisopropylamine / CH₂Cl₂ / 24 h / Ambient temperature

5: 99 percent / KF, pH 6.8 buffer / methanol / 17 h / Ambient temperature

With potassium fluoride; lithium aluminium tetrahydride; pH 6.8 buffer; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)90577-0