C₃₄H₅₀O₄Si

Base Information

Chemical Name:C₃₄H₅₀O₄Si
CAS No.:1374425-51-0
Molecular Formula:C₃₄H₅₀O₄Si
Molecular Weight:550.854
Hs Code.:

C<sub>34</sub>H<sub>50</sub>O<sub>4</sub>Si

Synonyms:C₃₄H₅₀O₄Si

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Chemical Property of C₃₄H₅₀O₄Si

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Technology Process of C₃₄H₅₀O₄Si

There total 22 articles about C₃₄H₅₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1374425-47-4
C₃₄H₄₆O₄Si

: 1374425-51-0
C₃₄H₅₀O₄Si

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201101629

Reference yield:

: C₁₃H₂₀O₅

: 1374425-51-0
C₃₄H₅₀O₄Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

5.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

6.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

7.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

7.3: 5 h / -78 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

9.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 °C / Inert atmosphere

10.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

12.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

13.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

13.2: 0.5 h / -78 - 20 °C / Inert atmosphere

14.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

15.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

16.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629

Reference yield:

: 1374425-20-3
C₁₃H₂₀O₃

: 1374425-51-0
C₃₄H₅₀O₄Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: ozone / dichloromethane / 3 h / -78 °C

2.2: 4 h / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

7.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

8.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

9.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

9.3: 5 h / -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

11.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

12.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

14.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

15.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

15.2: 0.5 h / -78 - 20 °C / Inert atmosphere

16.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

17.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

18.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629