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C26H31NO4S2

Base Information
  • Chemical Name:C26H31NO4S2
  • CAS No.:1265596-20-0
  • Molecular Formula:C26H31NO4S2
  • Molecular Weight:485.668
  • Hs Code.:
C<sub>26</sub>H<sub>31</sub>NO<sub>4</sub>S<sub>2</sub>

Synonyms:C26H31NO4S2

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Chemical Property of C26H31NO4S2
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Technology Process of C26H31NO4S2

There total 16 articles about C26H31NO4S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With C7H6O2*C20H27NOSi; In dichloromethane; at 0 ℃; for 20h; optical yield given as %de; stereoselective reaction;
DOI:10.1021/ol103064f
Guidance literature:
With C7H6O2*C20H27NOSi; In dichloromethane; at 0 ℃; for 20h; optical yield given as %de; stereoselective reaction;
DOI:10.1021/ol103064f
Guidance literature:
Multi-step reaction with 7 steps
1.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / -78 °C
1.2: 1 h / -78 °C
2.1: 1H-imidazole / dichloromethane / 1 h / 0 °C
3.1: dmap / acetonitrile / 17 h / 25 °C
4.1: ammonium chloride; magnesium / methanol / 24 h / 25 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
6.1: manganese(IV) oxide / dichloromethane / 4 h / 25 °C
7.1: C7H6O2*C20H27NOSi / dichloromethane / 20 h / 0 °C
With 1H-imidazole; dmap; manganese(IV) oxide; C7H6O2*C20H27NOSi; tetrabutyl ammonium fluoride; tert.-butyl lithium; ammonium chloride; magnesium; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; acetonitrile; pentane; 7.1: Aza-Michael Reaction;
DOI:10.1021/ol103064f
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