(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

Base Information

Chemical Name:(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt
CAS No.:20720-85-8
Molecular Formula:C₁₅H₁₁BrN₂O
Molecular Weight:315.169
Hs Code.:

Synonyms:(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

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Chemical Property of (Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

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Technology Process of (Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

There total 5 articles about (Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 79289-06-8
4-bromobenzophenone (E)-α-Chloroacetylhydrazone

: 20720-85-8
(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/ja00416a009

Reference yield: 32.0%

: 38582-62-6
4-bromobenzophenone (Z)-α-Chloroacetylhydrazone

: 20720-85-8
(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/ja00416a009

Reference yield:

: 28098-93-3,60664-67-7
4-bromo-benzophenone-(Z)-hydrazone

: 20720-85-8
(Z)-1-(p-bromophenylphenylmethylene)-3-oxo-1,2-diazetidinium inner salt

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / pyridine / CH₂Cl₂ / 0.25 h / Heating

2: 32 percent / 53percent sodium hydride / tetrahydrofuran / 24 h / Ambient temperature

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00416a009