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Technology Process of C29H34N2O9

C29H34N2O9

Base Information
  • Chemical Name:C29H34N2O9
  • CAS No.:1163143-75-6
  • Molecular Formula:C29H34N2O9
  • Molecular Weight:554.597
  • Hs Code.:
C<sub>29</sub>H<sub>34</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C29H34N2O9

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Chemical Property of C29H34N2O9
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Technology Process of C29H34N2O9

There total 1 articles about C29H34N2O9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C<sub>35</sub>H<sub>48</sub>N<sub>2</sub>O<sub>9</sub>Si
1163143-70-1

C35H48N2O9Si

C<sub>29</sub>H<sub>34</sub>N<sub>2</sub>O<sub>9</sub>
1163143-75-6

C29H34N2O9

Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/anie.200805724 DOI:10.1002/chem.201001060

Reference yield: 72.0%

(1S,5S,6S,8S)-2-benzyl-8-(tert-butyldimethylsiloxymethyl)-6-phenylsulfanyl-3,7-dioxa-2-azabicyclo[3.3.1]nonan-9-one
1163143-61-0

(1S,5S,6S,8S)-2-benzyl-8-(tert-butyldimethylsiloxymethyl)-6-phenylsulfanyl-3,7-dioxa-2-azabicyclo[3.3.1]nonan-9-one

C<sub>29</sub>H<sub>34</sub>N<sub>2</sub>O<sub>9</sub>
1163143-75-6

C29H34N2O9

C<sub>49</sub>H<sub>63</sub>N<sub>3</sub>O<sub>13</sub>Si
1163143-76-7

C49H63N3O13Si

Guidance literature:
(1S,5S,6S,8S)-2-benzyl-8-(tert-butyldimethylsiloxymethyl)-6-phenylsulfanyl-3,7-dioxa-2-azabicyclo[3.3.1]nonan-9-one; C29H34N2O9; With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;
With trifluorormethanesulfonic acid; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.200805724
upstream raw materials:

C35H48N2O9Si

Downstream raw materials:

C49H63N3O13Si

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